![]() This withdrawal shall become effective, if we fail to make the delivery within a reasonable extension period of at least four weeks. The delivery period shall be extended by force majeure or by all obstacles that by reasonable means cannot be influenced by us.Įxceeded delivery deadlines shall not entitle our customers to raise damage claims, but our customers may, if the delivery deadline has been exceeded by more than four weeks and this is exclusively due to our fault, withdraw from the contract by registered mail. We make an effort to keep the delivery deadlines defined by us, but since delivery does not only depend on us, we cannot make any binding promises. Delivery Deadlines, Delay and Non-Delivery Refrigerated goods are generally excluded from returns.Ĥ. Goods without defects may be returned to VWR International GmbH only with explicit consent and carriage paid. This stipulation does not entitle the customer to unilateral cancellation of a contract (order). #Antimony chloride plus#If, exceptionally, the purchase order (order) is cancelled by mutual consent without stipulation of a cancellation fee, the cancellation fee to be paid by the customer amounts to 20% or EURO 36.00 as basic sum plus value added tax. Orders by our customers, even when based on our offers, shall become binding only when confirmed in writing by us or when delivered.ĭue to rapid delivery basically no cancellation of orders is possible. Our offers and list prices are subject to alteration. We do not recognize the general conditions of our customers, even if we do not explicitly reject them in a specific case. If we act as agents of other companies, particularly of Merck KgaA, Darmstadt, the General Conditions of this company shall apply to the procured business (the so-called extended retention of title with regard to claims resulting from the sale of goods which remain the property of VWR until fully paid is, in view of the Austrian laws, considered as not agreed upon for deliveries to Austria) If a business has been concluded on the basis of the present General Terms and Conditions of Sale and Delivery, these will apply also to further business, even if no reference is made to them. By placing an order the customer irrevocably accepts the present conditions whose modification requires our written consent. particularly to industrial chemicals, reagents and diagnostic products as well as general laboratory supplies including equipment for the use of these products and consulting. Mabus - personal experience with the stuff it's pretty nasty to work with and without a glovebox or Schlenk line it's almost impossible to do any kind of proper reactions.The present general terms of sale and delivery apply to all business of VWR International GmbH, i.e.Ampouling is used for long term storage.Īntimony(III) chloride should be neutralized with a base then taken to a waste disposal center. Schlenk flasks are a common storage container. Contact with most protection gloves will cause them to darken.Īntimony compounds display moderate toxicity.Īntimony(III) chloride should be stored in dry air-tight containers, best in an inert atmosphere. ![]() Carr-Price test (detection of vitamin A and related carotenoids)Īntimony trichloride readily hydrolyzes in the presence of moisture to release hydrochloric acid which is very corrosive.Use a cold trap to prevent corrosive HCl and SbCl 3 fumes from getting sucked up in the pump and destroying it. The temperature at which vacuum sublimation begins is between 185-190 ☌. ![]() įor higher purity, it can be dried in a stream of HCl gas.Īntimony trichloride is best purified from old or partially hydrolyzed reagent by subliming it under vacuum and condense it on a cold finger. acid is removed via distillation, leaving in the flask impure SbCl 3, which can be purified by distilling it using a short-path distillation apparatus. ![]() hydrochloric acid, with a bit of hydrogen peroxide to speed up the reaction. The product is purified via sublimation under vacuum, using a cold finger.Īnother route involves reacting antimony(III) oxide with conc. Reaction must be performed in dry environment/atmosphere. It is soluble in ethers.Īntimony(III) chloride is sold by chemical suppliers, but it's difficult to get hold of due to its hazards.Īntimony(III) chloride can be prepared by reacting elemental antimony with dry chlorine gas. Visible hydrolysis is observed after 10 seconds of air exposure.Īntimony trichloride is a crystalline deliquescent solid, which readily hydrolyzes in moist air. Antimony(III) chloride rapidly hydrolyzes in moist air to give antimony oxychloride and hydrochloric acid. ![]()
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